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挤压温度对Mg-Sn合金显微组织和力学性能的影响
作者:
作者单位:

1.兰州理工大学 省部共建有色金属先进加工与再利用国家重点实验室,甘肃 兰州 730050;2.兰州理工大学 材料科学与工程学院,甘肃 兰州 730050;3.山西银光华盛镁业股份有限公司,山西 运城 043800;4.兰州兰石检测技术有限公司,甘肃 兰州 730050

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中图分类号:

TG146.22

基金项目:

甘肃省科技重大专项(22ZD6GA008);国家自然科学基金(52261027,52001152,51961021);甘肃省自然科学基金(22JR5RA251)


Effects of Extrusion Temperature on the Microstructure and Mechanical Properties of Mg-Sn Alloy
Author:
Affiliation:

1.State Key Laboratory of Advanced Processing and Recycling of Nonferrous Metals, Lanzhou Universing of Techology, Lanzhou 730050, China;2.School of Materials and Engineering, Lanzhou University of Technology, Lanzhou 730050, China;3.Shanxi Yinguang Huasheng Magnesium Industry Co., Ltd, Yuncheng 043800, China;4.Lanzhou Lanshi Testing Technology Co., Ltd, Lanzhou 730050, China

Fund Project:

The Major Science and Technology Project of Gansu Province (Grant No. 22ZD6GA008), National Natural Science Foundation of China (Nos. 52261027, 52001152 and 51961021), Gansu Natural Science Foundation (Nos. 22JR5RA251), Undergraduate Innovation and Entrepreneurship Training Program (Nos. DC20231482, DC20231188 and DC20231558).

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    摘要:

    本实验采用光学显微镜(OM)、X射线衍射(XRD)、电子背散射衍射(EBSD)、透射电子显微镜(TEM)和万能拉伸试验机研究了不同挤压温度(160、220和230 ℃)对晶粒异质结构Mg-7Sn合金显微组织和力学性能的影响。3种挤压合金均含有细小的动态再结晶晶粒和粗大的热加工晶粒。粗大晶粒和细小晶粒之间变形能力的差异导致了异质变形诱导应力(hetero-deformation induced stress, HDI)的形成。挤压合金形成了典型的(0001)α//ED基面织构,随着挤压温度的升高合金基面织构强度减弱,织构弱化主要归因于挤压温度的升高促进了合金动态再结晶以及非基面滑移的激活。挤压9E160合金在室温下表现出较高的抗拉强度(σb=341.83 MPa),这是由于HDI强化,细晶强化和高体积分数的纳米级Mg2Sn相沉淀强度导致。伴随挤压温度的升高促进了动态再结晶,合金的晶粒得到细化,合金的塑性也得到了进一步改善,合金塑性的改善归因于晶粒细化和非基面滑移系的激活。

    Abstract:

    The effects of different extrusion temperatures (160, 220 and 230 ℃) on the microstructure and mechanical properties of Mg-7Sn alloy with heterogeneous grain structure were investigated using optical microscope, X-ray diffractometer, electron backscatter diffractometer, transmission electron microscope, and a universal experimental tensile machine. All three extruded alloys contain fine dynamic recrystallized grains and coarse hot-worked grains. The difference in deformability between coarse and fine grains leads to the formation of hetero-deformation induced stress (HDI). The extruded alloys form a typical basal texture, and the texture strength of the basal texture is weakened with increasing extrusion temperature, which is mainly attributed to the fact that the increase in extrusion temperature promotes the dynamic recrystallization and the activation of non-basal slip. The extruded 9E160 alloy exhibits high tensile strength at room temperature (σb=341.83 MPa) due to HDI strengthening, fine grain strengthening and high volume fraction of nanoscale Mg2Sn phase precipitation strength. The increase in extrusion temperature facilitates dynamic recrystallization, resulting in grain refinement and further enhancement of the alloy's plasticity. The improved plasticity of the alloy can be attributed to both grain refinement and activation of non-basal slip systems.

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仝琳,姜静,毕广利,赵李斌,蒋春宏,陈体军,李元东.挤压温度对Mg-Sn合金显微组织和力学性能的影响[J].稀有金属材料与工程,2025,54(6):1507~1520.[Tong Lin, Jiang Jing, Bi Guangli, Zhao Libing, Jiang Chunhong, Chen Tijun, Li Yuandong. Effects of Extrusion Temperature on the Microstructure and Mechanical Properties of Mg-Sn Alloy[J]. Rare Metal Materials and Engineering,2025,54(6):1507~1520.]
DOI:10.12442/j. issn.1002-185X.20240069

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  • 收稿日期:2024-02-03
  • 最后修改日期:2024-05-08
  • 录用日期:2024-05-20
  • 在线发布日期: 2025-06-10
  • 出版日期: 2025-06-09