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纳米晶W粉的制备及烧结性能
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TF123.24 TF123.72

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Preparation of Nanocrystalline Tungsten Powder and Study of Its Sinterability
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    摘要:

    用高能球磨法制取纳米晶W粉,在真空炉内将此W粉分别进行无压和热压烧结成致密块体。利用扫描电镜,透射电镜,X-ray衍射仪等观测球磨过程中粉末粒度,形貌和结构的经及烧结块体的质量密度随温度的变化,并与普通粉的烧结性能作了比较。结果表明:脆性材料在高能球磨过程中不出现片层状结构,一直保持颗粒状结构,纳米晶超细W粉与普通W粉相比,由于颗粒和晶粒小,扩散系数高,表面能高,比表面原子烤多,晶格畸变严重,熔点

    Abstract:

    Nano-crystalline tungsten powder prepared by high - energy ball milling was consolidated without pressure and with pressure, respectively. The change of the particle size and morphology, and the relative density of the sintering compact as a function of consolidation temperature has been studied by SEM, TEM and X - ray diffraction. The sinterability of nanocrystalline tungsten powder is compared with that of coarse - grained tungsten powder. It is found that the usual layered structure does not develop during the high - energy ball milling of brittle materials. This work demonstrates that the sinterability of nanocrystalline powder is far superior to that of a coarse - grained one.Correspondent: Chen Xianfeng, Candidate for Master Degree, State Key Laboratory for Mechanical Behavior of Materials, Xi'arl Jlao'tong University, Xi'an 710049, P. R. China, Tel: 086 - 29 - 3268912

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陈献峰 张晖.纳米晶W粉的制备及烧结性能[J].稀有金属材料与工程,1998,(5):294~297.[Chen Xianfeng, Zhang Hui, Ding Bingjun. Preparation of Nanocrystalline Tungsten Powder and Study of Its Sinterability[J]. Rare Metal Materials and Engineering,1998,(5):294~297.]
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