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粉末冶金Ta合金中的隐性胞状结构
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TG146.4

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Hidden Cell Structure in Powder Metallurgy Ta Alloys
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    摘要:

    采用Ta-W-Hf预合金化粉末通过冷等静压成型、热等静压和高温退火工艺制备了Ta—W-Hf合金块材,讨论了热等静压和后续的高温退火处理对合金性能的影响。发现在低的热等静压温度下,材料具有较高的强度和硬度,但塑性较低;提高热等静压温度或进行高温退火处理,可以大幅度提高拉伸延伸率和断面收缩率,同时伴随着强度的降低。分析表明,产生这种现象的主要原因是合金中的氧元素在原料颗粒中分布不均匀,并保留在热等静压成形后的块体材料中,形成了一个无相变的隐性硬壳的胞状结构。高温退火处理可以消除这种结构。

    Abstract:

    Using pre-alloying Ta-W-Hf powder,Ta-W-Hf bulk alloys were prepared by means of CIP(cold isostatic press),HIP(hot isostatic press)and high temperature annealing.This paper is focused on the influences of HIP and high temperature annealing on the alloy performances.The results show that high strength,high hardness and low plasticity appear for the alloy after HIP at low temperature.The elongation and section shrinking would be largely improved and the strength would be decreased after HIP at high temperature or high temperature annealing due to the oxygen element's inhomogeneous distribution in the raw material particles and remaining in the bulk after HIP to form the hidden harden cell structures without phase change in these regions.These cell structures would disappear after high temperature annealing.

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张小明 张廷杰 胡忠武 李晴宇 谭栓斌 殷为宏.粉末冶金Ta合金中的隐性胞状结构[J].稀有金属材料与工程,2006,35(8):1243~1246.[Zhang Xiaoming, Zhang Tingjie, Hu Zhongwu, Li Qingyu, Tan Shuanbin, Yin Weihong. Hidden Cell Structure in Powder Metallurgy Ta Alloys[J]. Rare Metal Materials and Engineering,2006,35(8):1243~1246.]
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  • 收稿日期:2005-05-31
  • 最后修改日期:2006-04-28
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