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微量元素Nb、C强化W-Lu2O3复合材料的组织及性能研究
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合肥工业大学材料科学与工程学院,合肥工业大学材料科学与工程学院,合肥工业大学材料科学与工程学院,中科院等离子体物理研究所,合肥工业大学材料科学与工程学院,合肥工业大学材料科学与工程学院

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国际热核聚变实验堆(ITER)计划专项(2014GB121001);国家自然基金面上项目(51474083)


Research on microstructures and properties of W-Lu2O3 composite strengthened with Nb and C trace elements
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School of Material Science and Engineering,Hefei University of Technology,School of Material Science and Engineering,Hefei University of Technology,School of Material Science and Engineering,Hefei University of Technology,Institute of Plasma Physics,Chinese Academic Sciences,School of Material Science and Engineering,Hefei University of Technology,School of Material Science and Engineering,Hefei University of Technology

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    摘要:

    采用机械球磨和放电等离子体烧结制备了W-Lu2O3和W-Nb-C-Lu2O3合金,通过场发射扫描电子显微镜(FE-SEM)、能谱(EDS)和透射电子显微镜(TEM)研究分析了合金复合粉末的形貌、合金烧结体表面形貌和断口形貌;测定了合金的致密度、热导率、硬度和强度。实验结果表明:在W-Lu2O3的基础上添加微量Nb和C对钨合金晶粒细化、致密化和强度提高有着明显的效果,W-Nb-C-Lu2O3合金的致密度比W-Lu2O3提高了5.75%,达到了95.12%,晶粒尺寸由8~13 μm细化到2~5 μm,W-Nb-C-Lu2O3合金比W-Lu2O3合金的显微硬度和强度得到明显改善。

    Abstract:

    W-Lu2O3 and W-Nb-C-Lu2O3 composites were fabricated by mechanical milling and spark plasma sintering. The morphology of composite powders, surface and fracture surface morphology of the samples were characterized by field-emission scanning electron microscopy (FE-SEM), energy-dispersive spectroscopy (EDS) and transmission electron microscopy (TEM). The relative density, thermal conductivity, hardness and strength of the samples were also measured. Results revealed that the addition of trace Nb and C on the basis of W-Lu2O3 composite had an obvious effect on grain refinement, densification and strength. The relative density of W-Nb-C-Lu2O3 composite was 5.75% higher than W-Lu2O3 and reached 95.12%. The grain size of W-Nb-C-Lu2O3 composite was refined from 8~13 μm to 2~5 μm, and its microhardness and strength were obvious improved compared with W-Lu2O3 composite.

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张俊,罗来马,朱晓勇,罗广南,程继贵,吴玉程.微量元素Nb、C强化W-Lu2O3复合材料的组织及性能研究[J].稀有金属材料与工程,2017,46(9):2533~2538.[Zhang Jun, LuoLaima, Zhu Xiaoyong, Luo Guangnan, Cheng Jigui, Wu Yucheng. Research on microstructures and properties of W-Lu2O3 composite strengthened with Nb and C trace elements[J]. Rare Metal Materials and Engineering,2017,46(9):2533~2538.]
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  • 收稿日期:2015-05-25
  • 最后修改日期:2015-07-22
  • 录用日期:2015-09-07
  • 在线发布日期: 2017-11-29
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