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SPS烧结W-TaC的耐瞬态热冲击性能
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核工业西南物理研究院,核工业西南物理研究院,核工业西南物理研究院,核工业西南物理研究院,核工业西南物理研究院,大连理工大学

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国家自然科学基金(项目号11605044),中德科学基金(项目号GZ960)


Transient Thermal Shock Performance of Sintered W-TaC by SPS
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Southwestern Institute of Physics,Cheng Du,Southwestern Institute of Physics,Cheng Du,Southwestern Institute of Physics,Cheng Du,Southwestern Institute of Physics,Cheng Du,Southwestern Institute of Physics,Cheng Du,Dalian University of Technology,Da Lian

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    摘要:

    通过高能球磨方法制备了系列W-TaC混合粉末,采用放电等离子体烧结(SPS)制备出弥散强化W-TaC样品,并对W-TaC样品的密度、硬度和微观组织进行了分析。利用核工业西南物理研究院的60kW电子束材料测试平台(EMS-60)对烧结W-TaC的耐瞬态热冲击性能进行了测试,分别模拟了等离子体破裂和边缘局域模热负荷。实验后通过扫描电镜观察了样品加载区域的裂纹及熔化情况,通过透射电镜观察分析了材料的微结构特征。结果表明:W-TaC样品在热负荷作用下可以经受功率密度为740MW/m2、5ms的热冲击而不产生裂纹,但在功率密度为550MW/m2、100次1ms的热疲劳下会产生疲劳微裂纹。SEM和TEM分析表明TaC颗粒在钨晶粒内和晶粒间都有存在,而且TaC会与W形成共格相界和半共格晶界从而增强钨合金的强度。

    Abstract:

    Dispersion strengthened tungsten with tantalun carbide was prepared by Spark Plasma Sintering (SPS).High heat flux tests were performed with the electron beam device EMS-60 (60 kW Electron-beam Material-test Scenario) at Southwestern Institute of Physics.The polished tungsten surfaces were exposed to single shot disruption-like and repetitive ELM-like thermal shock loads at various absorbed energy densities.The thermal shock-induced damages were analysed by scanning electron microscope and the microstructure was observed by transmission electron microscope . The result show that no crack were detected on the tungsten surface when sample exposed to single shot thermal shock with absorbed energy density at 740MW/m2, crack appeared when sample exposed to repetitive thermal shock with absorbed power density at 550MW/m2. SEM and TEM images show that TaC particles disperse in tungsten grains interior including both intragranular and intergranular. This strategy including strengthening phase boundaries through coherent structure, strengthening grain boundaries through semi-coherent structure which leads to the excellent strengthen of W-TaC alloy plate.

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封范,练友运,刘翔,王建豹,王金,王英敏. SPS烧结W-TaC的耐瞬态热冲击性能[J].稀有金属材料与工程,2017,46(11):3544~3549.[Feng Fan, Lian Youyun, Liu Xiang, Wang Jianbao, Wang Jin, Wang Yingmin. Transient Thermal Shock Performance of Sintered W-TaC by SPS[J]. Rare Metal Materials and Engineering,2017,46(11):3544~3549.]
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  • 收稿日期:2016-08-26
  • 最后修改日期:2016-12-01
  • 录用日期:2016-12-06
  • 在线发布日期: 2017-12-13
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