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BP-GO-AgNPs复合涂层的制备及其抑菌性能研究
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中国民用航空飞行学院

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中国民用航空飞行学院科研基金面上项目(J2020-47),中国民用航空飞行学院研究生科研创新计划项目(X2020-9),微生物资源四川省科技资源共享服务平台


Preparation and antibacterial properties of BP-GO-AgNPs composite coating
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Civil Aviation Flight University of China

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    摘要:

    采用液相剥离技术对黑磷和氧化石墨烯进行分散,通过共价键作用制得BP-GO复合载体,经氧化还原反应在BP-GO复合载体表面原位还原AgNPs。探究了硝酸银含量、BP-GO含量比值对复合粉体性能影响,对比分析了相同条件下制备的BP-GO-AgNPs与GO-AgNPs复合涂层的抑菌性能。利用SEM、TEM分析表明,BP与GO成功分散,且BP-GO载体成功复合,同时AgNPs成功负载在载体表面,较优的AgNO3添加参数为3×10-4mol。XPS分析表明,BP与GO纳米片通过P-C、P-O-C的键合作用力联接,且AgNPs成功负载在载体表面,成功制得BP-GO-AgNPs复合粉体。Raman分析表明,复合粉体中BP-GO含量较优比值为1:1。抑菌结果表明,相同条件下,BP-GO-AgNPs复合涂层相较于GO-AgNPs复合涂层的抑菌效果更好。 关键词: BP;GO;AgNPs;抑菌涂层

    Abstract:

    The BP and GO were dispersed by liquid-phase stripping technique. By covalent bonding, BP-GO composite carrier was prepared. AgNPs were reduced in situ on the surface of BP-GO composite carrier by redox method.The effects of silver nitrate content and BP-GO content ratio on the properties of composite powders were investigated, and the antibacterial properties of BP-GO-AgNPs and GO-AgNPs composite coatings prepared under the same conditions were compared and analyzed.SEM and TEM analysis showed that BP and GO were successfully dispersed, BP-GO carrier was successfully combined, and AgNPs were successfully loaded on the carrier surface,with the optimal AgNO3 dosage parameter was 3×10-4mol.XPS analysis showed that BP-GO-AgNPs composite powders were successfully prepared by the joint of P-C and P-O-C, and the AgNPs were successfully loaded on the surface of the carrier.Raman analysis showed that the optimal ratio of BP-GO content in the composite powder was 1:1.The antibacterial results showed that the BP-GO-AgNPs composite coating had better antibacterial effect than the GO-AgNPs composite coating under the same conditions.

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张中波,李秀琴,李博轩. BP-GO-AgNPs复合涂层的制备及其抑菌性能研究[J].稀有金属材料与工程,2022,51(3):1017~1023.[Zhang Zhongbo, Li Xiuqin, Li Boxuan. Preparation and antibacterial properties of BP-GO-AgNPs composite coating[J]. Rare Metal Materials and Engineering,2022,51(3):1017~1023.]
DOI:10.12442/j. issn.1002-185X.20210212

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  • 收稿日期:2021-03-14
  • 最后修改日期:2021-04-16
  • 录用日期:2021-05-13
  • 在线发布日期: 2022-04-06
  • 出版日期: 2022-03-30