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电辅助成形工艺对TC4钛合金微观组织及拉伸性能的影响
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1.上海航天精密机械研究所,上海航天技术研究院;2.上海航天技术研究院;3.合肥工业大学材料科学与工程学院;4.上海航天精密机械研究所;5.合肥工业大学

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TG146.2+3

基金项目:

国家自然科学基金联合资助项目(项目号u23b20100);国家自然科学基金面上项目(项目号52475342);上海航天科技创新基金(SAST2021-071)


The Influence of Electric-assisted Forming Process on the Microstructure and Tensile Properties of TC4 Titanium Alloy
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Affiliation:

1.Shanghai Spaceflight Precision Machinery Institute, Shanghai, 201600;2.Hefei University of Technology

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国家自然科学基金联合资助项目(项目号u23b20100);国家自然科学基金面上项目(项目号52475342);上海航天科技创新基金(SAST2021-071)

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    摘要:

    本文通过对航空材料TC4钛合金在拉伸过程中通入不同频率的电流,以此来增加材料的流动应力并降低拉伸过程中的最大屈服强度。采用扫描电子显微镜来观察通电后材料组织的演变,以及试样的断口形貌。结合拉伸实验结果来分析电辅助成形工艺在拉伸过程中的影响。实验结果表明,随着脉冲电流密度的增加,α相的含量大大降低,β相含量大大增加其晶粒尺寸开始增大,在冷却过程中存在少量的马氏体相变生成的细小的针状α"相;随着电流密度的进一步增加,初生α相完全消失,β相进一步的长大,转变生成的α"相尺寸有所增大。在拉伸过程中,施加电流的瞬间试样的温度急剧上升,随着拉伸过程的进行,温度持续上升,且上升的速度不断加快,在断裂的瞬间达到峰值;峰值温度随着电流密度和脉冲频率的增加而增加,随着电流密度的升高,TC4钛合金的流动应力逐渐下降,塑性有所提升。SEM及TEM实验结果表明随着电流密度的增加,TC4钛合金板材拉伸断口中的韧窝显著加深,微观断口表面呈现出蜂窝状,韧窝周围出现撕裂棱,呈现出明显的韧性断裂的特征。与高温和常温拉伸对比,电辅助拉伸后材料内部的位错密度显著下降,位错较为平直且部分位错沿某一方向有序排列,这表明了脉冲电流对位错运动的促进作用。

    Abstract:

    This article investigates the effects of applying different frequencies of electric current during the tensile process of TC4 titanium alloy, a common aerospace material, to increase the material's flow stress and reduce the maximum yield strength during stretching. Scanning electron microscopy (SEM) was used to observe the evolution of the material's microstructure after electrical treatment, as well as the fracture morphology of the samples. The results of tensile tests were combined to analyze the impact of the electrically-assisted forming process during stretching. The experimental results indicate that as the pulse current density increases, the content of the α phase significantly decreases, while the content of the β phase greatly increases, with grain size beginning to enlarge. During the cooling process, a small amount of fine needle-like α" phase is formed due to the martensitic transformation. With further increases in current density, the primary α phase completely disappears, the β phase grows further, and the transformed α" phase size increases. During the stretching process, the temperature of the sample rises sharply at the moment of applying the current, continues to rise as the stretching process proceeds, and the rate of temperature increase accelerates, reaching a peak at the moment of rupture. The peak temperature increases with the increase of current density and pulse frequency. As the current density rises, the flow stress of TC4 titanium alloy gradually decreases, and its plasticity improves. SEM and TEM experimental results show that with the increase of current density, the dimples in the tensile fracture of TC4 titanium alloy sheets significantly deepen, the micro fracture surface presents a honeycomb-like appearance, and tear ridges appear around the dimples, showing distinct characteristics of ductile fracture. Compared with high-temperature and room-temperature stretching, the dislocation density inside the material significantly decreases after electrically-assisted stretching, the dislocations are relatively straight, and some dislocations are orderly arranged in a certain direction, indicating the promoting effect of pulse current on dislocation movement.

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彭赫力,祖清明,刘乐,刘海建,刘柏松,李萍.电辅助成形工艺对TC4钛合金微观组织及拉伸性能的影响[J].稀有金属材料与工程,,().[Peng Heli, Zu Qingming, Liu Le, Liu Haijian, Liu Baiong, Li Ping. The Influence of Electric-assisted Forming Process on the Microstructure and Tensile Properties of TC4 Titanium Alloy[J]. Rare Metal Materials and Engineering,,().]
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  • 收稿日期:2024-12-03
  • 最后修改日期:2025-04-23
  • 录用日期:2025-05-12
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