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Preparation and oxidation behavior of SiC coating for graphite materials
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Key Laboratory for Anisotropy and Texture of Materials of Ministry of Education ATM,Northeastern University,Key Laboratory for Anisotropy and Texture of Materials of Ministry of Education ATM,Northeastern University,Key Laboratory for Anisotropy and Texture of Materials of Ministry of Education ATM,Northeastern University,Key Laboratory for Anisotropy and Texture of Materials of Ministry of Education ATM,Northeastern University,Key Laboratory for Anisotropy and Texture of Materials of Ministry of Education ATM,Northeastern University

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    Abstract:

    SiC coating for protecting graphite materials against oxidation was prepared using SiC, Si and thermosetting phenolic resin as materials by vapor silicon infiltration process(VSI). SEM and XRD showed that a dense SiC coating was obtained with a C/SiC gradient inner layer acting as bonding layer and combined well with the outlayer SiC coating , the main phases of coating consisted of α-SiC, β-SiC and Si, and free Si was residual after the VSI process. The as-obtained SiC coating can effectively protect graphite after oxidation for 16 h at 1200 ℃ with a weight gain about 2.18 mg/cm2 in air and endured the thermal shock between 1000℃ and room temperature for 15 cycles with only 0.17wt% weight loss.

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[Jiang Yan, Ye Chaochao, Ru Hongqiang, Yue Xinyan, Wang Wei. Preparation and oxidation behavior of SiC coating for graphite materials[J]. Rare Metal Materials and Engineering,2018,47(S1):294~297.]
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History
  • Received:July 03,2017
  • Revised:July 03,2017
  • Adopted:January 29,2018
  • Online: October 22,2018
  • Published: